Skip to Content
Merck
All Photos(1)

Key Documents

G003777

GC Analysis of Triazine Herbicides on SLB®-5ms after SPME using 60 μm Carbowax® Fiber

application for SPME, suitable for GC

Sign Into View Organizational & Contract Pricing
All Photos(1)

About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

sample/matrix: Triazine herbicides at 2 ppb in 0.1M phosphate buffer, pH 7, with 25% NaCl, 9 mL in 10 mL screw cap vial
SPME fiber: 60 μM Carbowax (PEG) (57354-U)
extraction: 30 min direct immersion with agitation using CombiPal program
desorption process: 2 min at 250°C, splitless for 0.75 min then opened
column: SLB-5ms, 30 m x 0.25 mm I.D., 0.5μm film
oven: 60°C(1 min) to 150°C @ 25°C/min to 230°C @ 5°C/min (0.5 min)
inj. temp.: Splitless/split with 0.75mm ID liner and Merlin Microseal
detector: ITMS m/z=150-250 @ 0.5 μsec per scan, transfer line 310°C
carrier gas: Helium, 1mL/min constant flow

suitability

application for SPME

application(s)

agriculture
chemicals and industrial polymers
environmental
food and beverages

Legal Information

Carbowax is a registered trademark of Union Carbide
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description
    Prometon
    Simazine
    Atrazine
    Propazine
    Simetryn
    Ametryn
    Prometryn
    Terbutryn
    Cyanazine
    See All (9)

Choose from one of the most recent versions:

Certificates of Analysis (COA)

Lot/Batch Number

Sorry, we don't have COAs for this product available online at this time.

If you need assistance, please contact Customer Support.

Already Own This Product?

Find documentation for the products that you have recently purchased in the Document Library.

Visit the Document Library

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Contact Technical Service