Skip to Content
Merck
All Photos(1)

Key Documents

85433

Supelco

Silylating mixture III

for GC derivatization, LiChropur

Synonym(s):

N,O-Bis-(trimethylsilyl)-trifluoracetamid – chlorotrimethylsilane – 1-(trimethylsilyl)imidazole mixture, 1-(Trimethylsilyl)imidazole/BSTFA/TMCS 3/3/2 (v/v/v), N,O-Bis(trimethylsilyl)trifluoroacetamide/TMSIM/TMCS 3/3/2 (v/v/v)

Sign Into View Organizational & Contract Pricing


About This Item

UNSPSC Code:
12000000
NACRES:
NA.22

grade

for GC derivatization

Quality Level

form

liquid

quality

LiChropur

reaction suitability

reagent type: derivatization reagent
reaction type: Silylations

technique(s)

gas chromatography (GC): suitable

density

0.944 g/mL at 20 °C

storage temp.

2-8°C

SMILES string

C[Si](C)(C)Cl.C[Si](C)(C)Cl.C[Si](C)(C)n1ccnc1.C[Si](C)(C)n2ccnc2.C[Si](C)(C)n3ccnc3.C[Si](C)(C)O\C(=N\[Si](C)(C)C)C(F)(F)F.C[Si](C)(C)O\C(=N\[Si](C)(C)C)C(F)(F)F.C[Si](C)(C)O\C(=N\[Si](C)(C)C)C(F)(F)F

Looking for similar products? Visit Product Comparison Guide

General description

Silylating mixture III is one of the most potent general silylating agents used for gas chromatography derivatization, comprising of N,O-bis(trimethylsilyl)trifluoroacetamide (BSTFA), 1-(trimethylsilyl)imidazole (TMSIM) and trimethylchlorosilane (TMCS) in the ratio 3:3:2.

Other Notes

Powerful and general silylating mixture

Legal Information

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

related product

Signal Word

Danger

Hazard Classifications

Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Dam. 1 - Flam. Liq. 2 - Skin Corr. 1A - STOT SE 3

Target Organs

Respiratory system

Supplementary Hazards

Storage Class Code

3 - Flammable liquids

WGK

WGK 3

Flash Point(F)

37.4 °F

Flash Point(C)

3 °C


Choose from one of the most recent versions:

Certificates of Analysis (COA)

Lot/Batch Number

Don't see the Right Version?

If you require a particular version, you can look up a specific certificate by the Lot or Batch number.

Already Own This Product?

Find documentation for the products that you have recently purchased in the Document Library.

Visit the Document Library

Customers Also Viewed

Slide 1 of 2

1 of 2

C.E. Kientz et al.
Journal of Chromatography A, 355, 229-229 (1986)
J.M. Halket et al.
Journal of Chromatography A, 192, 434-434 (1980)

Articles

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Contact Technical Service