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Key Documents

54281-U

Supelco

Supelclean Ultra 2400

volume 3 mL, pkg of 54

Synonym(s):

Supelclean™ Ultra

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

product line

Supelclean™

Quality Level

100

composition

bed A, 270 mg (Supelclean™ PSA, Discovery® C18, and Spherical Carbon)
bed B, 225 mg (Z-Sep)

packaging

pkg of 54

technique(s)

solid phase extraction (SPE): suitable

volume

3 mL

matrix active group

C18 bonding
PSA bonding
carbon bonding

application(s)

food and beverages

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General description

This multi-bed solid phase extraction (SPE) cartridge was designed for the cleanup of extracts of difficult matrices such as dry commodities (tea, spices, coffee, etc.) prior to pesticide residue analysis, typically performed by GC/MSMS and LC/MS/MS. These types of samples can contain pigments and oils, and may not be sufficiently cleaned using a standard QuEChERS cleanup.
The top bed consists of a mixture of PSA/C18 and a graphitized, spherical carbon. PSA removes acidic interferences, C18 retains some hydrophobic interferences, and carbon removes pigments. The variety of carbon used in this cartridge was engineered to remove sufficient pigmentation while allowing for better recoveries of compounds with planar structures. The bottom bed of the cartridge contains Z-Sep, which is a zirconia-coated silica. Z-Sep removes oily residues, and provides additional pigment removal.
The cartridge can be used for cleanup of acetonitrile extracts to be analyzed by either GC or HPLC.

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Pictograms

CorrosionExclamation mark
GHS05,GHS07

Signal Word

Danger

Hazard Statements

H317 - H318

Hazard Classifications

Eye Dam. 1 - Skin Sens. 1

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
17023503
17023502
17023501
16781702
16781701

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Articles

Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS after Cleanup with Dual-Layer SPE Cartridge

Pesticide residue testing of turmeric and other (dried) spices is challenging due to their complex compositions and high matrix. An efficient SPE clean-up can be achieved by a new Dual-layer cartridge.

Analysis of Pesticide Residues in Ginger Powder Using QuEChERS Extraction and Clean-up with a Novel Dual Layer SPE Cartridge

The odor and pungency of ginger is due to the presence of terpenes, gingerols and shogaols. These compounds contribute to the highly complex matrix of ginger, which subsequently presents a challenge in low level analyses of contaminants. A novel 2-layer SPE cartridge efficiently reduces background for pesticide determination.

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