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SU860097

Supelco

Flacons Headspace, haut à vis, fond arondi (flacon seul)

volume 20 mL, clear glass vial, thread for 18, O.D. × H 22.5 mm × 75.5 mm, pkg of 100 ea

Synonyme(s) :

Screw cap rounded bottom headspace vial

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About This Item

Code UNSPSC :
41122001
Nomenclature NACRES :
NB.11

Matériaux

clear glass vial
round bottom

Caractéristiques

closure type screw top vial

Conditionnement

pkg of 100 ea

D.E. × H

22.5 mm × 75.5 mm

Volume

20 mL

Raccords

thread for 18

Compatibilité

for use with CTC PAL (Varian, Gerstel, Atas, Shimadzu)

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Description générale

Ces flacons requièrent un bouchon spécial ayant un filetage de 18 mm. Les bouchons filetés standards 18-400 ne s′adapteront pas à ces flacons. Les références de bouchons disponibles pour ces flacons sont les suivantes : SU860101(avec PTFE/silicone, épaisseur 1,3 mm), SU860102 (avec PTFE/butyl, épaisseur 1,6 mm), et SU860103 (avec PTFE/silicone, épaisseur 1,5 mm). Ces bouchons sont faits en acier inoxydable et ils sont magnétiques.

Application

Headspace vial may be used for the following:
  • In the determination of partition coefficient of ethyl acetate in water at 0° C from independent analyses of the total amount of ethyl acetate present in the vial, by automatic equilibrium headspace gas chromatography and vapor phase calibration (VPC).
  • It may be used in the analysis of volatile polar residual solvents present in pharmaceutical products, during development and optimisation of headspace SPME method by GC-MS.
  • It may also be used in the isotopic analysis of 18O in the leaf water of C3 and C4 grasses, during establishing a grassland signature in veins, as it was found that grasses with different photosynthetic pathway have different interveinal differences.
  • It may also find application, in investigating metabolism by Pseudomonas fluorescens of volatile haloaliphatic hydrocarbons like 1,2-dichloroethane and 1,2-dichloropropane, which are some of the major contaminants of underground aquifers.

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Determination of partition coefficients by automatic equilibrium headspace gas chromatography by vapor phase calibration.
Welter KBC and Bichler C.
Chromatographia, 34 (5-8), 235-240 (1992)
B R Helliker et al.
Proceedings of the National Academy of Sciences of the United States of America, 97(14), 7894-7898 (2000-07-08)
We show that 18O evaporative enrichment of bulk leaf water in grass species can be significantly more enriched than predicted by the Craig-Gordon model, with C4 grasses considerably more enriched than C3 grasses. Our results suggest that the unanticipated 18O
P A Vandenbergh et al.
Applied and environmental microbiology, 54(10), 2578-2579 (1988-10-01)
A Pseudomonas fluorescens strain designated PFL12 was isolated from soil and water that were contaminated with various chloroaliphatic hydrocarbons. The isolate was able to metabolize 1,2-dichloroethane, 1,1,2-trichloroethane, 1,2-dichloropropane, 2,2-dichloropropane, and trichloroethylene.
C C Camarasu
Journal of pharmaceutical and biomedical analysis, 23(1), 197-210 (2000-07-18)
A solid-phase microextraction (SPME) method has been developed and optimized for the polar residual solvent determination in pharmaceutical products. Five different polymer-coated fibers were investigated and the Carboxen/polydimethylsiloxane was found to be the most sensitive for all components. Two Headspace

Protocoles

High performance, reliability, and reproducibility of HS-SPME in combination with GC/MS for the determination of VOCs in water was proven in an interlaboratory trial. The new ISO 17943 using HS-SPME is an improvement on existing official methods for this determination in terms of sensitivity and selectivity.

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