54240-U
Supel™-Select SCX SPE Tube
bed wt. 30 mg, volume 1 mL, pk of 100
About This Item
Produits recommandés
Matériaux
PE frit (20 μm)
polypropylene hardware
Qualité
MS Friendly
Composition
bed wt., 30 mg
Conditionnement
pk of 100
Technique(s)
solid phase extraction (SPE): suitable
Superficie
160-420 m2/g
Volume
1 mL
Matrice
Sulfonic acid functionalized hydrophilic modified styrene polymer particle platform
Groupe de la matrice active
sulfonic acid phase
Taille des particules
50-70 μm
Dimension de pores
80-200 Å pore size
Application(s)
food and beverages
Technique de séparation
ion exchange
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Description générale
Sample Matrix Compatibility: Aqueous solutions (biological fluids, water)
- Sulfonic acid functionalized hydrophilic modified styrene polymer
- Developed for the extraction of a highly broad range of compounds from aqueous samples
- Retention predominately based on ion-exchange; however, because the phase is hydrophilic modified, it is amenable to polar compounds as well.
View related article: Isolation and LC-MS Characterization of Illicit Bath Salts in Urine
Caractéristiques et avantages
- Excellent sample prep performance at a lower price
- Amenable to generic methodology - save time, money, and headache during method development
- Greater capacity allows for smaller bed weights = smaller elution volumes = time savings in sample processing
- Resistance to overdrying allows for more robust methdology
- Low UV and MS extractables for lower background and greater sensitivity
- Stringent production and QC guidelines offer greater lot-to-lot, tube-to-tube, and well-to-well consistency for improved accuracy and precision
Informations légales
Mention d'avertissement
Warning
Mentions de danger
Conseils de prudence
Classification des risques
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
Organes cibles
Respiratory system
Code de la classe de stockage
11 - Combustible Solids
Classe de danger pour l'eau (WGK)
WGK 3
Point d'éclair (°F)
Not applicable
Point d'éclair (°C)
Not applicable
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Articles
The combination of ion-exchange SPE with the HILIC HPLC separation provides a novel approach for the testing of problematic bath salt compounds.
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
Protocoles
Separation of 3,4-Methylenedioxypyrovalerone HCl (MDPV) solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Buphedrone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; 3-Fluoromethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Butylone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Ethylone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; 4-Fluoromethcathinone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Mephedrone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Methylone hydrochloride, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material; Methedrone hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material
Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.
Chromatograms
application for HPLCNotre équipe de scientifiques dispose d'une expérience dans tous les secteurs de la recherche, notamment en sciences de la vie, science des matériaux, synthèse chimique, chromatographie, analyse et dans de nombreux autres domaines..
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