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Key Documents

794-0438

GC Analysis of Volatiles in Water on SPB®-1 after SPME using 100 μm PDMS Fiber

suitable for GC, application for SPME

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About This Item

technique(s)

gas chromatography (GC): suitable
solid phase microextraction (SPME): suitable

test parameters

SPME fiber: polydimethylsiloxane, 100 μm (57300-U)
extraction: 5 min immersed in water with rapid stirring
column: SPB-1, 10 m × 0.20 mm I.D., 1.2 μm (24134-U)
oven: 40 °C ( 0.75 min) to 160 °C at 20 °C/min
inj. temp.: 230 °C, splitless (closed 3 min)
detector: FID, 260 °C
carrier gas: helium, 40 cm/sec
sample: 50ppb each analyte in 1.8 mL saturated salt water

suitability

application for SPME

application(s)

environmental
food and beverages

Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description

    1,1-Dichloroethylene
    Trichlorofluoromethane
    Ethylbenzene
    trans-1,3-Dichloropropene
    1,4-Dichlorobenzene
    Carbon tetrachloride
    Tetrachloroethylene
    Chlorobenzene
    Dibromochloromethane
    trans-1,2-Dichloroethene, analytical standard
    2-Chloroethyl vinyl ether
    Chloroethane
    Bromomethane
    1,4-Dichlorobutane
    Methylene chloride
    1,1,1-Trichloroethane
    1,1,2,2-Tetrachloroethane
    1,2-Dichloroethane
    Chloromethane
    Chloroform
    cis-1,3-Dichloropropene
    Trichloroethylene
    1,1-Dichloroethane
    Toluene
    Bromoform
    1,1,2-Trichloroethane
    Benzene
    1,2-Dichlorobenzene
    1,2-Dichloropropane
    1,3-Dichlorobenzene
    Bromodichloromethane
    Vinyl chloride
    See All (32)

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