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Key Documents

808645

TSKgel® Chelate-5PW (10 µm) HPLC Columns

L x I.D. 7.5 cm × 7.5 mm, iminodiacetic acid phase

Sinónimos:

TSKgel® Chelate-5PW HPLC Column and Guardgel Kit

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About This Item

UNSPSC Code:
41115700
eCl@ss:
32110501

product name

TSKgel® Chelate-5PW HPLC Column, phase iminodiacetic acid, L × I.D. 7.5 cm × 7.5 mm, 10 μm particle size

material

stainless steel

product line

TSKgel®

manufacturer/tradename

Tosoh Chelate-5PW, 08645

extent of labeling

20 μmol/mL resin ligand density

parameter

≤20% organic solvent
≤3 M salt concentration
≤45 °C temperature
1.2 mL/min flow rate
10 bar max. pressure

technique(s)

HPLC: suitable

L × I.D.

7.5 cm × 7.5 mm

matrix

polymer particle platform

matrix active group

iminodiacetic acid phase

particle size

10 μm

pore size

1000 Å

operating pH

2-12

compatibility

technique used for affinity HPLC

separation technique

affinity

General description

High efficiency, resin-based TSKgel affinity columns (10 μm particles) separate or purify many enzymes and other proteins.

TSKgel Chelate-5PW columns utilize the tendency of iminodiacetic acid (IDA) to form a complex with metal ions, such as Zn2+, Ni2+ and Cu2+. The column is loaded with divalent metal ions by chelation. Peptides and proteins containing histidine residues will normally adsorb to these chelated ions at neutral pH. The retained compounds can be eluted with buffer containing imidazole or glycine. The key to making successful use of this retention mechanism is the proper selection of metal ions for chelation and the elution buffer to desorb the analytes. In general, Cu2+, interacts better with proteins; however, resolution is usually enhanced with Zn2+. A gradient mobile phase containing increasing imidazole or glycine concentrations is used to elute the retained compounds. Alternatively, a decreasing pH gradient can be used for elution purposes as well.

Applications include: immunoglobulins, transferrin, lectins, milk proteins, membrane proteins and peptides.

Recommended products

Discover LiChropur reagents ideal for HPLC or LC-MS analysis

Legal Information

TSKgel is a registered trademark of Tosoh Corporation

guard column


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