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Merck

375934

Sigma-Aldrich

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide

≥95%, with 1% tert-Butyldimethylchlorosilane

Sinónimos:

MTBSTFA+TBDMSCl, 99:1, N-Methyl-N-tert-butyldimethylsilyltrifluoroacetamide, MTBSTFA + 1% TBDMSCl, Silylating mixture VI

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About This Item

Fórmula empírica (notación de Hill):
C9H18F3NOSi
Número de CAS:
Peso molecular:
241.33
Beilstein/REAXYS Number:
3606546
MDL number:
UNSPSC Code:
12352001
PubChem Substance ID:
NACRES:
NA.22

product name

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, ≥95%

Quality Level

assay

≥95%

form

liquid

contains

1% TBDMSCl

storage temp.

−20°C

SMILES string

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3

InChI key

QRKUHYFDBWGLHJ-UHFFFAOYSA-N

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Application

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-butyldimethylchlorosilane is commonly used for the preparation of N-tert-butyldimethylsilyl ethanolamines resulting from the hydrolysis of nitrogen mustards. It is also used for selective O-silylation of N,O-diacylhydroxyl amines.

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Referencia del producto
Descripción
Precios

pictograms

FlameExclamation mark

signalword

Warning

Hazard Classifications

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Storage Class

3 - Flammable liquids

wgk_germany

WGK 3

flash_point_f

113.0 °F - closed cup

flash_point_c

45 °C - closed cup

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter


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Organometallics, 23, 2157-2161 (2004)
Xiaodong Huang et al.
Analytical chemistry, 80(1), 107-114 (2007-12-07)
This work describes an approach to differential metabolomics that involves stable isotope labeling for relative quantification as part of sample analysis by two-dimensional gas chromatography/mass spectrometry (GCxGC/MS). The polar metabolome in control and experimental samples was extracted and differentially derivatized
Claude Schummer et al.
Talanta, 77(4), 1473-1482 (2008-12-17)
In this study, MTBSTFA and BSTFA, which are among the preferred derivatization reagents for silylation were both tested on derivatization of six different groups of polar chemicals to get information about usefulness in terms of sensitivity and specificity of both
A Royer et al.
Journal of chromatography. A, 1108(1), 129-135 (2006-01-31)
An analytical method has been developed for the determination of residues of ethephon (2-chloroethyl phosphonic acid) in drinking and surface water. The procedure is based on de-ionisation with an anion/cation-exchange resin, solid phase extraction by means of anion-exchange polystyrene-divinylbenzene extraction
Xiaowei Wang et al.
Analytica chimica acta, 753, 57-63 (2012-10-31)
A sample preparation method for the determination of hydroxylated polycyclic aromatic hydrocarbons (OH-PAHs) in sediment samples was developed using gas chromatography-mass spectrometry (GC-MS). Dispersive liquid-liquid microextraction (DLLME) with derivatization was performed following the subcritical water extraction (SWE) that provided which

Artículos

Results of a study involving the ability few Fluka silylating reagents to form GC-MS-compatible trimethylsilylmethyl derivatives of NSAIDs

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