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  • Derivatization and template-guided ligation of oligodeoxyribonucleotides using cyanogen bromide and N-substituted morpholines.

Derivatization and template-guided ligation of oligodeoxyribonucleotides using cyanogen bromide and N-substituted morpholines.

Origins of life and evolution of the biosphere : the journal of the International Society for the Study of the Origin of Life (2001-09-07)
Z A Shabarova, O A Fedorova, N G Dolinnaya, M B Gottikh
ABSTRACT

Cyanogen bromide has been found to induce the template-guided condensation of oligonucleotides only in the presence of N-substituted morpholines. Based on 31P, 1H and 13C NMR spectroscopy data, the mechanism of the phosphomonoester group activation by cyanogen bromide in N-substituted morpholine buffers is suggested. It has also been shown that BrCN can be used for the synthesis of oligonucleotide derivatives in aqueous solution.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Cyanogen bromide solution, 3.0 M in methylene chloride
Sigma-Aldrich
Cyanogen bromide solution, 5.0 M in acetonitrile