GC Analysis of 1-Phenylethylamine Enantiomers (N-Acetyl Derivatives) on Astec® CHIRALDEX™ B-DM
CONDITIONS
column
Astec CHIRALDEX B-DM, 30 m x 0.25 mm I.D., 0.12 μm (77023AST)
oven
135 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 30 psi
injection
1 μL, 80:1 split
sample
3 mg/mL in methylene chloride
peak 1: S(-)-1-phenylethylamine (N-acetyl derivative)
peak 2: R(+)-1-phenylethylamine (N-acetyl derivative)
Description
Analysis Note
Can reverse elution order by using CHIRALDEX G-PN, or by using the N-TFA derivative on the B-DM column.
Legal Information
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC