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Evaluation of gallic acid loaded zein sub-micron electrospun fibre mats as novel active packaging materials.

Food chemistry (2013-07-23)
Yun Ping Neo, Simon Swift, Sudip Ray, Marija Gizdavic-Nikolaidis, Jianyong Jin, Conrad O Perera
ABSTRACT

The applicability of gallic acid loaded zein (Ze-GA) electrospun fibre mats towards potential active food packaging material was evaluated. The surface chemistry of the electrospun fibre mats was determined using X-ray photon spectroscopy (XPS). The electrospun fibre mats showed low water activity and whitish colour. Thermogravimetric analysis (TGA) and Attenuated Total Reflectance-Fourier Transform Infrared (ATR-FTIR) spectroscopy revealed the stability of the fibre mats over time. The Ze-GA fibre mats displayed similar rapid release profiles, with Ze-GA 20% exhibiting the fastest release rate in water as compared to the others. Gallic acid diffuses from the electrospun fibres in a Fickian diffusion manner and the data obtained exhibited a better fit to Higuchi model. L929 fibroblast cells were cultured on the electrospun fibres to demonstrate the absence of cytotoxicity. Overall, the Ze-GA fibre mats demonstrated antibacterial activity and properties consistent with those considered desirable for active packaging material in the food industry.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Gallic acid, 97.5-102.5% (titration)
Sigma-Aldrich
Zein
Supelco
Gallic acid, certified reference material, TraceCERT®