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Merck
  • Lipase-catalyzed enantioselective transesterification of prochiral 1-((1,3-dihydroxypropan-2-yloxy)methyl)-5,6,7,8-tetrahydroquinazoline-2,4(1H,3H)-dione in ionic liquids.

Lipase-catalyzed enantioselective transesterification of prochiral 1-((1,3-dihydroxypropan-2-yloxy)methyl)-5,6,7,8-tetrahydroquinazoline-2,4(1H,3H)-dione in ionic liquids.

Chirality (2017-11-16)
Renata Kołodziejska, Renata Studzińska, Hanna Pawluk
摘要

The application of ionic liquids as solvents for transesterification of prochiral pirymidine acyclonucleoside using lipase (EC 3.1.1.3) Amano PS from Burkholderia cepacia (BCL) is reported. The effect of using medium reaction, acyl group donor, and temperature on the activity and enantioselectivity of BCL was studied. From the investigated ionic solvents, the hydrophobic ionic liquid [BMIM]PF

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Sigma-Aldrich
1,3-亚丙基丙烯, 99%
Sigma-Aldrich
正丁酸乙烯酯, contains 20 ppm 4-methoxyphenol as stabilizer, ≥99.0% (GC)
Sigma-Aldrich
1-己基-3-甲基咪唑四氟硼酸盐, ≥97.0% (HPLC)