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  • Method development for separating organic carbonates by ion-moderated high-performance liquid chromatography.

Method development for separating organic carbonates by ion-moderated high-performance liquid chromatography.

Journal of separation science (2016-11-03)
Anuja Bhalkikar, Chris M Marin, Chin Li Cheung
摘要

An ion-moderated partition high-performance liquid chromatography method was developed for the separation and identification of common organic carbonates. The separation of organic carbonates was achieved on an ion exclusion column with an exchangeable hydrogen ion. An isocratic, aqueous mobile phase was used for elution and detection was performed with a refractive index detector. The developed method was validated for specificity, linearity, limits of detection and quantification, precision and accuracy. All calibration curves showed excellent linear regression (R

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Sigma-Aldrich
硫酸, 99.999%
Sigma-Aldrich
碳酸二乙酯, anhydrous, ≥99%
Sigma-Aldrich
羟甲基二氧杂戊环酮