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  • Synthesis of LiYF4:Yb, Er upconversion nanoparticles and its fluorescence properties.

Synthesis of LiYF4:Yb, Er upconversion nanoparticles and its fluorescence properties.

Journal of nanoscience and nanotechnology (2014-04-18)
Liming Zhang, Zhixin Wang, Zhuoxuan Lu, Kai Xia, Yan Deng, Song Li, Chuanxiang Zhang, Yuanfu Huang, Nongyue He
ABSTRACT

LiYbF4:Yb, Er nanoparticles have been successfully synthesized by thermal decomposition of multiple trifluoroacetic acid salts. The SEM and TEM results show the size of the LiYF4:Yb, Er nanoparticles is about 100 nm in diagonal line, and the morphology of the LiYF4:Yb, Er nanoparticles is highly uniform with octahedral structure. Under the excitation of 980 nm, the LiYF4:Yb, Er nanoparticles have higher upconversion luminescence efficiency compared with that of NaYF4:Yb, Er. The results indicate that the as-prepared LiYbF4:Yb, Er nanoparticles may have potential applications in bio-probes and displays.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Lithium fluoride, Precipitated, 99.995%
Sigma-Aldrich
Lithium fluoride, powder, -300 mesh
Sigma-Aldrich
Lithium fluoride, ≥99.99% trace metals basis
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Yttrium, chips, 99.9% trace rare earth metals basis
Sigma-Aldrich
Lithium fluoride, powder, <100 μm, ≥99.98% trace metals basis
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Ytterbium, powder, ≥99.9% trace rare earth metals basis
Sigma-Aldrich
Lithium-6Li fluoride, 95 atom % 6Li, 99% (CP)
Sigma-Aldrich
Yttrium sputtering target, diam. × thickness 2.00 in. × 0.25 in., 99.9% trace metals basis