GC Analysis of Amphetamines in Plasma on SLB^®-5ms (20 m x 0.18 mm I.D., 0.36 μm) after SPME using 100 μm PDMS Fiber, Fast GC Analysis

SPME fiber

100 μm PDMS (57300-U)

extraction

headspace, 300 rpm stirring at 75 °C for 15 min

column

SLB-5ms, 20 m x 0.18 mm I.D. x 0.36 μm (28576-U)

oven

75 °C (1 min), 10 °C/min to 190°C, 25 °C/min to 300 °C (4 min)

MSD interface

300 °C

carrier gas

helium, 0.7 mL/min. constant

liner

0.75 mm I.D. SPME