跳转至内容
Merck

LC/MS (TOF) Analysis of Opioids and Opiate-Dependence Management Drugs on Ascentis® Express HILIC

LC/MS (TOF) Analysis of Opioids and Opiate-Dependence Management Drugs on Ascentis® Express HILIC application for HPLC

材料

分析柱

产品编号
说明
价格

53934-U

Ascentis® Express HILIC, 2.7 μm HPLC色谱柱

2.7 μm particle size, L × I.D. 5 cm × 2.1 mm

標準

产品编号
说明
价格

A-009

6-乙酰吗啡标准液 溶液

1 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

C-006

可待因标准液 溶液

1 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

H-004

氢吗啡酮标准液 溶液

1 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

A-053

6-乙酰可待因标准液 溶液

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

H-003

氢可酮标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

M-005

吗啡标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

O-002

羟考酮标准液 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

流動相成分

产品编号
说明
价格

70221

甲酸铵

eluent additive for LC-MS, LiChropur™, ≥99.0%

CONDITIONS

column

Ascentis Express HILIC, 5 cm x 2.1 mm I.D., 2.7 μm particles (53934-U)

mobile phase

2 mM ammonium formate in 90:10 (v:v) acetonitrile:water

flow rate

0.3 mL/min

column temp.

55 °C

detector

TOF/MS

injection

2 μL

sample

400 ng/mL in acetonitrile

说明

分析報告

The rapid analysis by HPLC with TOF-MS detection of seven opioids is shown here using an Ascentis Express HILIC column. Cerilliant CRMs were used to ensure reliable MS identification and quantification.

法律資訊

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

Chromatogram Search

Related Product Categories

HPLC ColumnsGC Columns & AccessoriesTLC Plates & AdsorbentsSolid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS