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GC Analysis of Wieland-Miescher Ketone Enantiomers on Astec® CHIRALDEX G-TA

GC Analysis of Wieland-Miescher Ketone Enantiomers on Astec® CHIRALDEX™ G-TA suitable for GC

Materials

analytical column

Product No.
Description
Pricing

Astec® CHIRALDEX G-TA Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

standard

Product No.
Description
Pricing

(±)-8a-Methyl-3,4,8,8a-tetrahydro-1,6(2H,7H)-naphthalenedione

98%

CONDITIONS

column

Astec CHIRALDEX G-TA, 30 m x 0.25 mm I.D., 0.12 μm (73033AST)

gradient

110 °C, 5 °C/min to 160 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 35 psi

sample

peak 1: S(+)-Wieland-Miescher Ketone
peak 2: R(-)-Wieland-Miescher Ketone

Description

Analysis Note

Elution order reversal on CHIRALDEX G-BP.

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC