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54217-U

Supelco

Supelclean™ ENVI-Carb™ II/PSA SPE Tube

bed A 500 mg (Supelclean™ ENVI-Carb-II SPE), bed B 500 mg (Supelclean™ PSA SPE), volume 20 mL, pk of 20

Synonym(s):

Carbon/PSA SPE cartidge, 20 mL

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

material

PE frit (20 μm porosity)
polypropylene hardware

Quality Level

100

composition

bed A, 500 mg (Supelclean™
ENVI-Carb-II SPE)
bed B, 500 mg (Supelclean™
PSA SPE)

packaging

pk of 20

technique(s)

solid phase extraction (SPE): suitable

volume

20 mL

matrix active group

PSA phase
carbon phase

application(s)

food and beverages

separation technique

ion exchange
reversed phase

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General description

Retention Mechanism: Reversed-phase and anion-exchange
Sample Matrix Compatibility: Organic or aqueous solutions

  • Dual layer SPE tube that contains both Supelclean ENVI-Carb (upper layer) & PSA (lower layer) SPE sorbents (separated by PE frit)
  • Developed to offer superior clean up when conducting multi-residue pesticide analysis from food (e.g. agricultural products, meats, etc.).
  • ENVI-carb has a strong affinity towards planar molecules, and can isolate/remove pigments (e.g., chlorophyll and carotinoids) and sterols commonly present in foods and natural products
  • Supelclean PSA is a polymerically bonded, ethylenediamine-N-propyl phase that contains both primary and secondary amines
  • Supelclean PSA has a strong affinity and high capacity for fatty acids, organic acids, and some polar pigments and sugars
  • Tested for superior cleanliness using GC-FID and GC-MS

Legal Information

ENVI-Carb is a trademark of Sigma-Aldrich Co. LLC
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Signal Word

Danger

Hazard Statements

H317,H318,H373

Hazard Classifications

Eye Dam. 1 - Skin Sens. 1 - STOT RE 2 Inhalation

Target Organs

respiratory tract irritation

Storage Class Code

11 - Combustible Solids

WGK

WGK 1

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
16941901
15317101
12793302
12793301
12182102

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Articles

Solid Phase Extraction: Ion Exchange Methodology

SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

Solid Phase Extraction: Reversed-Phase Methodology

Reversed-phase interaction will retain most molecules with hydrophobic character; it is very useful for extracting analytes that are very diverse in structure within the same sample.

Protocols

Solid Phase Extraction: Normal Phase Methodology

Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.

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