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GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astecยฎ CHIRALDEXโ„ข G-DP

GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-DP suitable for GC

Materials

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Astecยฎ CHIRALDEXโ„ข G-DP Capillary GC Column

L ร— I.D. 30 m ร— 0.25 mm, df 0.12 ฮผm

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GC Analysis of Amphetamine Enantiomers (N-Trifluoroacetyl Derivative) on Astecยฎ CHIRALDEXโ„ข G-PN

suitable for GC

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D-Amphetamine hemisulfate salt solution

1.0 mg/mL in methanol, analytical standard, for drug analysis

DL-Amphetamine sulfate salt

D-Amphetamine hemisulfate salt

DL-Amphetamine hydrochloride

analytical standard

CONDITIONS

column

Astec CHIRALDEX G-DP, 30 m x 0.25 mm I.D., 0.12 ฮผm (78033AST)

oven

140 ยฐC

detector

FID, 250 ยฐC

inj. temp.

250 ยฐC

carrier gas

helium, 2.7 mL/min., constant flow

injection

1 ฮผL, 80:1 split

liner

4 mm I.D., FocusLiner

sample

4 mg/mL each compound in methylene chloride
peak 1: d-amphetamine (N-TFA derivative)
peak 2: l-amphetamine (N-TFA derivative)

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๋ถ„์„ ๋ฉ”๋ชจ

Elution order reversal (l,d) by using CHIRALDEX G-PN, 130ยฐC (see G005053).

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Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC