GCによる2-ブタノールエナンチオマー (O-トリフルオロアセチル誘導体) の分析、Astec® CHIRALDEX™ G-TA
CONDITIONS
column
Astec CHIRALDEX G-TA, 30 m x 0.25 mm I.D., 0.12 μm (73033AST)
gradient
30 °C (5 min), 5 °C/min to 110 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 30 psi
injection
1 μL, 80:1 split
sample
peak 1: R(-)-2-butanol (O-TFA derivative)
peak 2: S(+)-2-butanol (O-TFA derivative)
詳細
アナリシスノート
Elution order reversal by using the O-Acetyl derivative on CHIRALDEX G-TA.
法的情報
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC