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KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
core: palladium

functional group



Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:
  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit Components Also Available Separately

Product No.

  • 764175P(Cy3) Pd G3, 97%

  • 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%

  • 804274XPhos Pd G4, 95%

  • 804282SPhos Pd G4

  • 804290RuPhos Pd G4

  • 804975DTBPF-Pd-G3

  • 900349cataCXium Pd G4

  • 900522Toluene, anhydrous, ZerO2®, 99.8%

  • 900631Ethylene glycol, anhydrous, ZerO2®, 99.8%

  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%

  • 9006391-Butanol, anhydrous, ZerO2®, 99.8%

  • 900641Methanol, anhydrous, ZerO2®, 99.8%

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%

  • 900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%

  • 221171Pinacol, 98%

  • 473294Bis(pinacolato)diboron, 99%

  • 754242Tetrahydroxydiboron, 95%

  • B34656Biphenyl, ReagentPlus®, 99.5%

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm

  • Z742110KitAlysis 24-well reaction block replacement film

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Signal Word


Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1

Target Organs


Supplementary Hazards

Storage Class Code

3 - Flammable liquids



Flash Point(F)

1.4 °F

Flash Point(C)

-17 °C

Certificate of Analysis

Certificate of Origin

Quotes and Ordering


KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.


Catalyst Screening followed by TLC-MS for Reaction Progress Analysis using KitAlysis™

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