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Sigma-Aldrich

KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
core: palladium

functional group

phosphine

Application

Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:
  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit Components Also Available Separately

Product No.
Description
SDS

  • 764175P(Cy3) Pd G3, 97%

  • 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%

  • 804274XPhos Pd G4, 95%

  • 804282SPhos Pd G4

  • 804290RuPhos Pd G4

  • 804975DTBPF-Pd-G3

  • 900349cataCXium Pd G4

  • 900522Toluene, anhydrous, ZerO2®, 99.8%

  • 900631Ethylene glycol, anhydrous, ZerO2®, 99.8%

  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%

  • 9006391-Butanol, anhydrous, ZerO2®, 99.8%

  • 900641Methanol, anhydrous, ZerO2®, 99.8%

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%

  • 900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%

  • 221171Pinacol, 98%

  • 473294Bis(pinacolato)diboron, 99%

  • 754242Tetrahydroxydiboron, 95%

  • B34656Biphenyl, ReagentPlus®, 99.5%

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm

  • Z742110KitAlysis 24-well reaction block replacement film

See All (21)

Signal Word

Danger

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1

Target Organs

Kidney

Supplementary Hazards

Storage Class Code

3 - Flammable liquids

WGK

WGK 3

Flash Point(F)

1.4 °F

Flash Point(C)

-17 °C

Certificate of Analysis

Enter Lot Number to search for Certificate of Analysis (COA).

Certificate of Origin

Enter Lot Number to search for Certificate of Origin (COO).

SDS

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