US EPA Method 8270 (PAH only): GC Analysis of PAHs on SLB^®-5ms

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

50 °C (1 min), 10 °C/min to 325 °C (5 min)

inj. temp.

300 °C

detector

FID, 365 °C

MSD interface

300 °C

scan range

m/z 45-450

carrier gas

helium, 0.9 mL/min., constant

injection

1 μL, splitless (1 min)

liner

3.8 mm I.D., straight

sample

Each analyte at 10 μg/mL in methylene chloride