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Expedient synthesis of sulfinamides from sulfonyl chlorides.

The Journal of organic chemistry (2007-01-16)
Michael Harmata, Pinguan Zheng, Chaofeng Huang, Maria G Gomes, Weijiang Ying, Kanok-On Rayanil, Kanok-On Ranyanil, Gayatri Balan, Nathan L Calkins
ABSTRACT

Sulfinamides were synthesized from sulfonyl chlorides using a procedure involving in situ reduction of sulfonyl chlorides. The reaction is broad in scope and easy to perform.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
Sulfuryl chloride, 97%
Sigma-Aldrich
Sulfuryl chloride solution, 1.0 M in methylene chloride