8.53029
Boc-Glu(OcHx)-OH
Novabiochem®
Synonym(s):
Boc-Glu(OcHx)-OH, N-α-t.-Boc-L-glutamic acid γ-cyclohexyl ester
About This Item
Recommended Products
Quality Level
product line
Novabiochem®
Assay
≥98% (TLC)
form
powder
reaction suitability
reaction type: Boc solid-phase peptide synthesis
manufacturer/tradename
Novabiochem®
mp
54-57 °C
application(s)
peptide synthesis
functional group
carboxylic acid
storage temp.
2-30°C
InChI
1S/C16H27NO6/c1-16(2,3)23-15(21)17-12(14(19)20)9-10-13(18)22-11-7-5-4-6-8-11/h11-12H,4-10H2,1-3H3,(H,17,21)(H,19,20)/t12-/m0/s1
InChI key
FDNMLANBNJDIRG-LBPRGKRZSA-N
General description
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] J. P. Tam, et al. (1979) Tetrahedron Lett., 42, 4033.
Linkage
Analysis Note
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in methanol): -9.0 - -7.0 °
Purity (TLC(0811)): ≥ 98 %
Purity (DC (0157)): ≥ 98 %
Solubility (1 mmole in 2 ml DMF): clearly soluble
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Legal Information
Storage Class Code
11 - Combustible Solids
WGK
WGK 3
Flash Point(F)
Not applicable
Flash Point(C)
Not applicable
Certificates of Analysis (COA)
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Protocols
The most popular reagent for cleavage of peptides from Boc-based resins is anhydrous HF. Of all the cleavage procedures HF appears to be the most versatile and least harmful to a wide variety of peptides synthesized on Boc-based resins.
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