Acetaldehyde, methanol, and ethanol analysis by headspace gas chromatography.

Acetaldehyde, methanol, and ethanol analysis by headspace gas chromatography.

Journal of analytical toxicology (1980-01-01)

R M Anthony, C A Sutheimer, I Sunshine

ABSTRACT

This report describes a headspace procedure suitable for the gas chromatographic assay of acetaldehyde, methanol, ethanol and various other volatile substances in biological samples. Carbopack B coated with 5% Carbowax 20-M is compared to Carbopack C coated with 0.2% Carbowax 1500. Assay range, linearity and precision are reported for the Carbopack B material.

MATERIALS

Product Number

Brand

Product Description

82762

Supelco

Methanol, analytical standard

10436

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ X, 40-60 mesh, bottle of 10 g

10439-U

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ X, 120-400 mesh, bottle of 50 g

10257

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ C, 60-80 mesh, bottle of 10 g

10437-U

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ X, 60-80 mesh, bottle of 10 g

10258

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ C, 80-100 mesh, bottle of 10 g

29535-U

Supelco

Carbopack^™ B, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., preconditioned, pkg of 10 ea

30136-U

Supelco

Carbopack^™ B, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., unconditioned, pkg of 10 ea, matrix Carbopack^™

30135-U

Supelco

Carbopack^™ B, stainless steel TD tube, O.D. × L 1/4 × 3 1/2, unconditioned, pkg of 10 ea

28686-U

Supelco

FLM Carbopack^™ X Deactivated Stainless Steel TD Tube, preconditioned, pkg of 10 tubes, O.D. × L 1/4 in. (6.35 mm) × 3 1/2 in. (89 mm)

29754-U

Supelco

Carbopack^™ B, O.D. × L 1/4 in. × 3 1/2 in., glass TD tube, fritted, Sealed with Brass Endcaps, preconditioned, pkg of 10 ea

20273

Supelco

Carbopack^™ Adsorbent, matrix Carbopack^™ B, 60-80 mesh, bottle of 10 g

11809

Supelco

Coated GC Packing, phase 1% SP^®-1510, matrix 60/80 Carbopack B support, bottle of 15 g

29537-U

Supelco

Carbopack^™ X, glass TD tube, fritted, O.D. × L 1/4 in. × 3 1/2 in., preconditioned, pkg of 10 ea