GC Analysis of QA Test Mix on SLB^®-5ms, Three Different Phase Lots

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

110 °C (14 min), 15 °C/min to 325 °C (15 min)

inj. temp.

250 °C

detector

FID, 360 °C

carrier gas

helium, 30 cm/sec @ 110 °C

injection

1.0 μL 100:1 split

liner

4 mm I.D. split, cup design

sample

Nonpolar Column Test Mix, each analyte at 500 μg/mL in methylene chloride