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Method development for separating organic carbonates by ion-moderated high-performance liquid chromatography.

Journal of separation science (2016-11-03)
Anuja Bhalkikar, Chris M Marin, Chin Li Cheung
RÉSUMÉ

An ion-moderated partition high-performance liquid chromatography method was developed for the separation and identification of common organic carbonates. The separation of organic carbonates was achieved on an ion exclusion column with an exchangeable hydrogen ion. An isocratic, aqueous mobile phase was used for elution and detection was performed with a refractive index detector. The developed method was validated for specificity, linearity, limits of detection and quantification, precision and accuracy. All calibration curves showed excellent linear regression (R

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Sigma-Aldrich
Acide sulfurique, 99.999%
Sigma-Aldrich
Diethyl carbonate, anhydrous, ≥99%
Sigma-Aldrich
4-(Hydroxymethyl)-1,3-dioxolan-2-one