LC/MS (TOF) Analysis of 2C Amine Drugs of Abuse on Ascentis® Express HILIC
Materialien
Analytische Säule
Produkt-Nr.
Beschreibung
Preisangaben
Komponente der mobilen Phase
Produkt-Nr.
Beschreibung
Preisangaben
Standard
Produkt-Nr.
Beschreibung
Preisangaben
4-Brom-2,5-Dimethoxyphenethylamin -hydrochlorid -Lösung
1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®2C-B-FLY -hydrochlorid -Lösung
1 mg/mL in acetonitrile: water (9:1), ampule of 1 mL, certified reference material, Cerilliant®2,5-Dimethoxy-4-(n-propylthio)-phenethylamin -hydrochlorid -Lösung
1.0 mg/mL in acetonitrile: water (9:1) (as free base), ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express HILIC, 5 cm x 2.1 mm I.D., 2.7 μm particles (53934-U)
mobile phase
2 mM ammonium formate in 90:10 (v:v) acetonitrile:water
flow rate
0.4 mL/min
pressure
943 psi (65 bar)
column temp.
35 °C
detector
TOF/MS
injection
2 μL
sample
300 ng/mL in acetonitrile
Beschreibung
Hinweis zur Analyse
The 2C amines are a family of illicit, psychedelic phenethylamines. The term "2C" refers to the two carbon atoms between the benzene ring and the amino group in the parent molecular structure. A rapid separation of four 2C amine compounds is shown here on an Ascentis Express HILIC column with TOF-MS detection. Cerilliant CRMs were used to ensure reliable MS identification and quantification.
Rechtliche Hinweise
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany