- C-acylations of polymeric phosphoranylidene acetates for C-terminal variation of peptide carboxylic acids.
C-acylations of polymeric phosphoranylidene acetates for C-terminal variation of peptide carboxylic acids.
Organic letters (2007-02-20)
Adeeb El-Dahshan, Steffen Weik, Jörg Rademann
PMID17305347
RESUMEN
C-Acylations of polymer-supported 2-phosphoranylidene acetates ("linker reagents") with protected amino acids yielded 2-acyl-2-phosphoranylidene acetates as flexible intermediates for the C-terminal variation of carboxylic acids: peptidyl-2,3-diketoesters, peptidyl vinyl ketones, peptidyl-2-ketoaldehydes, and 1,3-diamino-2-hydroxy-propanes were obtained as products. [reaction: see text]
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